Online Course
Application of Spectroscopic Methods in Molecular Structure Determination
Indian Institute of Technology Madras and NPTEL via Swayam
-
109
-
- Write review
Overview
INTENDED AUDIENCE: BSc Chemistry final year, MSc Chemistry and PhD Chemistry students.
PREREQUISITES : A good background knowledge in organic chemistry/stereochemistry necessary
INDUSTRY SUPPORT : Scientists in Chemical and Pharma industry will be interested. Beneficial to scientists working chemistry in R&D labs, national labs etc
Syllabus
COURSE LAYOUT
Week 1: Introduction to spectroscopic methods – Nuclear magnetic resonance spectroscopy (NMR), spin ½ nuclei, 1H and 13C-NMR spectroscopy, FT-NMR method. Chemical shifts, spin spin coupling, spin-spin splitting pattern recognition for structure elucidation, coupling constants.Week 2: 1H NMR spectroscopy, Second order effects in NMR spectrum, AB and AA’BB’, ABC spin systems. Solving simple structure elucidation problems with 1H and 13C NMR spectroscopyWeek 3: Stereochemistry determination using NMR techniques. Study of dynamic processes by NMR spectroscopy – examples from organic and organometallic chemistryWeek 4: Mass Spectrometry – various ionization methods – EI, CI, ESI and MALDI methods, fragmentation patterns of simple organic molecules, Use of HRMS.Week 5: Mass spectrometry – fragmentation patterns of simple organic molecules (continued), solving structure elucidation problems using mass spectrometry.Week 6: Infra-red spectroscopy – basic concepts, experimental methods, functional group analysis and identification using IR spectroscopy, structural effects on vibrational frequencyWeek 7: UV-Vis spectroscopy, electronic transitions in organic molecules, selection rules, application of Beer Lambert law, qualitative and quantitative analysis by UV-Vis spectroscopy.Week 8: Solving structure elucidation problems using multiple spectroscopic data (NMR, MS, IR and UV-Vis).Taught by
S. Sankararaman
Tags
Related Courses
-
Introduction to Molecular Spectroscopy
University of Manchester
4.2 -
Molecular Spectroscopy: A Physical Chemist's Perspective
Indian Institute of Technology Bombay, NPTEL
-
ARPIT 2020 : Online Refresher Course In Chemistry For Higher Education
AICTE, Shri Guru Tegh Bahadur Khalsa College
-
Chemistry and Physics of Surfaces and Interfaces
Indian Institute of Technology Kanpur, NPTEL
-
Analytical Techniques
All India Institute of Medical Sciences, New Delhi, UGC, CEC
-
Structure, Stereochemistry and Reactivity of Organic Compounds and Intermediates: A Problem-solving Approach
Indian Institute of Technology, Kharagpur, NPTEL
Reviews
0.0 rating, based on 0 reviews